反应 #544432
ord-f2b98b38f7104dd097424cd92de5d75b
反应方程式
tributyl phosphate
ammonium lactate
→
ammonium lactate
lactic acid
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1温度The reaction mixture was heated for 0.5 hour at 110–118° C.
实验过程
The procedure described in Example 1 was followed except that 7.57 g of a 70% solution of ammonium lactate was combined with 50 g tributyl phosphate. The reaction mixture was heated for 0.5 hour at 110–118° C. and a reduced pressure of 4.5–5.5 mm Hg, resulting in a conversion of about 97% from ammonium lactate to lactic acid.