反应 #543581

ord-247eb979cb984156839a1b613e26b8cd

反应方程式

CCNC(=O)Nc1ccccc1O
N-ethyl-N′-(2-hydroxyphenyl)urea
COc1ccccc1N=C=O
1-isocyanato-2-methoxybenzene
CNC
dimethylamine
CN(C)C(=O)Nc1ccccc1O
subtitled compound
收率 54.0%
CN(C)C(=O)Nc1ccccc1O
N′-(2-hydroxyphenyl)-N,N-dimethylurea
收率 54.0%

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

The subtitled compound was prepared using the procedure as described for Example 25 for N-ethyl-N′-(2-hydroxyphenyl)urea from 1-isocyanato-2-methoxybenzene and dimethylamine (2M solution in THF). Yield 54%.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07186718B2uspto-grants-2007_03