反应 #543569

反应方程式

4-oxo-piperidine-1-carboxylic acid tert-butyl ester

tert-butylcarbazate

→

4-(tert-Butoxycarbonyl-hydrazono)-piperidine-1-carboxylic acid tert-butyl ester

溶剂

hexane

反应条件

后处理

1. 1
   过滤The precipitate is filtered off
2. 2
   其他dried under vacuum

实验过程

A mixture of 0.15 mole of 4-oxo-piperidine-1-carboxylic acid tert-butyl ester (commercially available) and 0.15 mole of tert-butylcarbazate in 250 ml of hexane is stirred for 18 h at RT. The precipitate is filtered off and dried under vacuum. M. p. 172–174° C.

来源