反应 #531791

反应方程式

Mercaptopropionic acid

Triphenylmethylchloride

→

3-(tritylthio)propionic acid

收率 95.7%

溶剂

methylene chloride

反应条件

后处理

1. 1
   其他were carried out at room temperature
2. 2
   过滤was gathered by filtration
3. 3
   其他the solid components obtained here
4. 4
   其他were dried under reduced pressure

实验过程

Mercaptopropionic acid 12 (3.14 g) was dissolved in 50 ml of methylene chloride. Triphenylmethylchloride 13 (8.36 g) was added to that, and 19-hour reactions were carried out at room temperature. The precipitate generated through the reactions was gathered by filtration, and the solid components obtained here were dried under reduced pressure, to form 9.86 g of 3-(tritylthio)propionic acid 14, which is a white solid.

来源