反应 #53152

ord-1739ac8b4e434a479c80560d9bd0f09c

反应方程式

CCOC(=C1C(=O)Nc2ccc([N+](=O)[O-])cc21)c1ccccc1
3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone
Nc1ccc(CN2CCC(Cc3ccccc3)CC2)cc1
4-(4-phenylmethyl-piperidino)methyl-aniline
→
O=C1Nc2ccc([N+](=O)[O-])cc2/C1=C(/Nc1ccc(CN2CCC(Cc3ccccc3)CC2)cc1)c1ccccc1
(Z)-3-{1-[4-(4-phenylmethyl-piperidinomethyl)-phenylamino]-1-phenyl-methylidene}-5-nitro-2-indolinone

反应物

CCOC(=C1C(=O)Nc2ccc([N+](=O)[O-])cc21)c1ccccc1
3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone
Nc1ccc(CN2CCC(Cc3ccccc3)CC2)cc1
4-(4-phenylmethyl-piperidino)methyl-aniline

试剂

无

溶剂

CN(C)C=O
DMF

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

Prepared analogously to Example 89 from 3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone and 4-(4-phenylmethyl-piperidino)methyl-aniline in DMF.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US06855710B2uspto-grants-2005_02