反应 #5223

ord-dcadfe0e1eca4e47a8b88dad58fe8309

溶剂

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    workup.STIRRINGThereafter, the mixture was stirred at room temperature for 19 hours

实验过程

2-Aminoethanol (13.76 g, 225.3 mmol) was dissolved in CHCl3 (750 ml). To the solution was added dropwise palmitoyl chloride (15.48 g, 56.3 mmol) with stirring under ice cooling. Thereafter, the mixture was stirred at room temperature for 19 hours.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05243035uspto-grants-1993_09