反应 #50428

ord-d9402f9cd14742bf8acde96329546880

溶剂

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他The same procedure as in Preparation Example 3
  2. 2
    其他were used and that reaction

实验过程

The same procedure as in Preparation Example 3 was effected except that 1441 g (10 mols) of L-lactide, 1140 g (10 mols) of ε-caprolactone and 10 ml of a toluene solution containing 0.26 g of stannous octoate, and 5 g of lauryl alcohol were used and that reaction was carried out at 160° C. for 10 hours, thereby obtaining a lactic acid-hydroxycaproic acid copolymer (hereinafter referred to as "PCLA1").

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: USRE034984uspto-grants-1995_06