反应 #487409

ord-f8d184a5c3014a92bc4fb77c554723dc

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他The reaction

实验过程

To a solution of 50.0 g (220 mmol, Aldrich) of 3-bromocinnamic acid in 1 L sieve-dried methanol (Burdick & Jackson), stirred at 0° C., was added dropwise a solution of acidic methanol (prepared by the addition of 2.5 mL acetyl chloride to 250 mL methanol). The reaction

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05827868uspto-grants-1998_10