反应 #487409
ord-f8d184a5c3014a92bc4fb77c554723dc
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他The reaction
实验过程
To a solution of 50.0 g (220 mmol, Aldrich) of 3-bromocinnamic acid in 1 L sieve-dried methanol (Burdick & Jackson), stirred at 0° C., was added dropwise a solution of acidic methanol (prepared by the addition of 2.5 mL acetyl chloride to 250 mL methanol). The reaction