反应 #470371

反应方程式

N-methoxymethyl-N-methylpyrrolidinium chloride

N-Methoxymethyl-N-Methylpyrrolidinium Chloride

potassium hexafluorophosphate

→

white solid

N-Methoxymethyl-N-Methylpyrrolidinium hexafluorophosphate

溶剂

water

反应条件

后处理

1. 1
   其他separated out
2. 2
   workup.ADDITIONdichloromethane was thereafter added to the mixture for extraction
3. 3
   洗涤The organic layer was washed with 120 g of water six times
4. 4
   其他dried

实验过程

A 20.0 g quantity of N-methoxymethyl-N-methylpyrrolidinium chloride prepared in Example 10 was dissolved in 120 g of water, and 22.2 g of potassium hexafluorophosphate was added to the solution, whereupon a white solid separated out. The mixture was stirred for 30 minutes, and dichloromethane was thereafter added to the mixture for extraction. The organic layer was washed with 120 g of water six times and then dried, affording 25.1 g of a white solid as the desired product.

来源