反应 #470370

反应方程式

sodium trifluoroacetate

N-methoxymethyl-N-methylpyrrolidinium chloride

N-Methyl-N-Methoxymethylpyrrolidinium Chloride

→

colorless liquid

N-Methoxymethyl-N-Methylpyrrolidinium trifluoroacetate

溶剂

methanol

反应条件

后处理

1. 1
   浓缩concentrated in a vacuum
2. 2
   其他dried in a vacuum
3. 3
   workup.DISSOLUTIONThe residue was dissolved in 500 ml of dichloromethane
4. 4
   过滤followed by filtration with a membrane
5. 5
   过滤filter
6. 6
   浓缩concentration in a vacuum
7. 7
   其他drying

实验过程

A 14.94 g quantity of sodium trifluoroacetate was dissolved in 100 g of methanol, and 18.20 g of N-methoxymethyl-N-methylpyrrolidinium chloride was added to the solution at room temperature. The mixture was stirred for 1 hour, concentrated in a vacuum and dried in a vacuum using a vacuum pump. The residue was dissolved in 500 ml of dichloromethane, followed by filtration with a membrane filter, concentration in a vacuum and drying, affording 26.52 g of a colorless liquid as the desired product.

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