反应 #470367

反应方程式

Methoxymethylpyrrolidine

dimethyl carbonate

→

desired product

收率 60.0%

N-Methoxymethyl-N-Methylpyrrolidinium Methyl carbonate

收率 60.0%

反应条件

后处理

1. 1
   其他reacted at 120° C. for 24 hours
2. 2
   过滤The resulting solids were filtered off
3. 3
   洗涤washed with dimethyl carbonate
4. 4
   其他The solids were dried in a vacuum

实验过程

Methoxymethylpyrrolidine (10.00 g) and 117.39 g of dimethyl carbonate were placed into an autoclave and reacted at 120° C. for 24 hours. The resulting solids were filtered off and washed with dimethyl carbonate. The solids were dried in a vacuum, giving 10.70 g of the desired product.

来源