反应 #465953

ord-c4b88dc8fc2f43d4a6be06585468b591

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

300 mmoles of t-butanol, 100 mmoles of 1-hexanol and 2.5 g of Ti-Si-catalyst powder are stirred in a 100 ml autoclave at a pressure of 40 bar N2 and a temperature of 150° C. over a period of 17 h, 17% of n hexanol were converted into hexyl t-butyl ether with a selectivity of 90%.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US06297180B1uspto-grants-2001_10