反应 #459085

ord-cd09d6336b994885940ef8d9e1c38257

反应方程式

C=CC(N)=O
acrylamide
C=CC(=O)O
acrylic acid
[Na+].[OH-]
NaOH
O=S(=O)([O-])OOS(=O)(=O)[O-].[NH4+].[NH4+]
ammonium persulfate
→
C=CC(=O)O.C=CC(N)=O
Acrylamide Acrylic Acid

反应物

C=CC(N)=O
acrylamide
C=CC(=O)O
acrylic acid
[Na+].[OH-]
NaOH
O=S(=O)([O-])OOS(=O)(=O)[O-].[NH4+].[NH4+]
ammonium persulfate

试剂

无

溶剂

O
Water
O
water
O
water

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他to react with a catalyst mixture
  2. 2
    温度at refluxing temperature

实验过程

In a reactor similar to Example 1, a monomer mixture containing 622.0 grams of acrylamide, 54.8 grams of acrylic acid, 168.4 grams of 10% NaOH and 182 grams of water was allowed to react with a catalyst mixture containing 1.3 grams of ammonium persulfate in 198 grams of water at refluxing temperature. Water was used as a solvent in amount of 1934.0 grams

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US04088530uspto-grants-1978_05