反应 #452477
ord-22fea30183c04db69593e05118e5f118
反应方程式
acrylonitrile
2-methoxyphenylpiperazine
→
product
收率 91.7%
3-[4-(2-Methoxyphenyl)piperazin-1-yl]propionitrile
收率 91.7%
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他the solvent was evaporated in vacuo
实验过程
A solution of acrylonitrile (1.06 g, 20 mmol) in ethanol (50 ml) was added to a stirred solution of 2-methoxyphenylpiperazine (3.84 g, 20 mmol) in ethanol (100 ml). After 18 h, the solvent was evaporated in vacuo to give the product (4.5 g) as a white solid.