反应 #452433

反应方程式

4-dimethylamino-1-cyclohexanone ethylene ketal

→

title compound

收率 100.0%

4-dimethylamino-1-cyclohexanone

收率 100.0%

溶剂

formic acid

反应条件

后处理

1. 1
   温度at reflux for 18 hours
2. 2
   温度The reaction mixture was then cooled to ambient and the volatiles
3. 3
   其他removed under reduced pressure

实验过程

4.96 gm (26.8 mMol) 4-dimethylamino-1-cyclohexanone ethylene ketal were dissolved in 50 mL formic acid and the solution stirred at reflux for 18 hours. The reaction mixture was then cooled to ambient and the volatiles removed under reduced pressure to give 3.78 gm (100%) of the title compound.

来源