反应 #452418
ord-f0c77084774e4de89993e1a0f961c8ef
反应方程式
levulinic acid
cesium hydroxide
→
CESIUM LEVULINATE
溶剂
反应条件
温度
65°CELSIUS
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他to obtain complete solution
- 2过滤The solution is filtered through No
- 3过滤40 filter paper
- 4其他to remove dust, etc. The solution
- 5其他is then evaporated on a hot plate to 200 g
- 6其他, which gives
- 7浓缩a 2 molar concentration, and it
实验过程
46.9 gr. of 99% pure levulinic acid is sluurried in 100 cc. distilled water. 97.3 g. of a 4.22 molar, pure cesium hydroxide solution is added and the temperature is raised to 65° C. to obtain complete solution. The solution is filtered through No. 40 filter paper to remove dust, etc. The solution is then evaporated on a hot plate to 200 g., which gives a 2 molar concentration, and it is then bottled.