反应 #417926

反应方程式

sodium hydroxide

33

methyl 4-(undec-4Z-enyloxy)benzoate

→

white solid

收率 98.1%

4-(undec-4Z-enyloxy)benzoic acid

收率 98.1%

溶剂

methanol

反应条件

后处理

1. 1
   温度The solution is refluxed for 20 hours
2. 2
   其他After evaporating off the solvent
3. 3
   萃取extracted with DCM

实验过程

550 μL of 1 N sodium hydroxide solution (550 μmol) are added portionwise to 109 mg of 33 (358 μmol) in methanol (4 mL). The solution is refluxed for 20 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 102 mg of a white solid are obtained, i.e. a yield of 98%.

来源