反应 #417924

反应方程式

sodium hydroxide

29

methyl 2-(undec-4Z-enyloxy)benzoate

→

yellow oil

收率 99.5%

2-(undec-4Z-enyloxy)benzoic acid

收率 99.5%

溶剂

methanol

反应条件

后处理

1. 1
   温度The solution is refluxed for 24 hours
2. 2
   其他After evaporating off the solvent
3. 3
   萃取extracted with DCM

实验过程

500 μL of 1 N sodium hydroxide solution (500 μmol) are added portionwise to 80 mg of 29 (263 μmol) in methanol (3 mL). The solution is refluxed for 24 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 76 mg of a yellow oil are obtained, i.e. a yield of 99%.

来源