反应 #417906
ord-dd72aa198be14ac5966dd35f8a2286f6
反应方程式
Desmorapid
n-butyl isocyanate
isocyanate
→
Isopropyl butylcarbamate
反应条件
温度
60°CELSIUS
详细条件
See reaction.notes.procedure_details.
后处理
- 1温度Thereafter, cooling
- 2其他the product was obtained as a clear liquid
实验过程
In a 250 ml round-bottomed flask, 0.02 g of Desmorapid Z, 31.1 g of n-butyl isocyanate were initially introduced and heated to 60° C. Thereafter, 18.9 g of isopropanol were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, cooling was effected and the product was obtained as a clear liquid.