反应 #4140

反应方程式

1-(4-Bromo-2-nitrophenyl)-1,2,3,4-tetrahydroquinoline

ethanol

→

product

收率 100.0%

1-(4-Bromo-2-aminophenyl)-1,2,3,4-tetrahydroquinoline

收率 100.0%

溶剂

benzene

反应条件

后处理

1. 1
   过滤The mixture was filtered
2. 2
   其他the filtrate was evaporated at 50° C. under vacuum

实验过程

1-(4-Bromo-2-nitrophenyl)-1,2,3,4-tetrahydroquinoline (11.6 g, 0.035 mole) was dissolved in benzene (125 ml), and ethanol added (75 ml), followed by 1% platinum-on-charcoal (0.40 g). The mixture was shaken under an initial pressure of 56 psi for 6.5 hours. The mixture was filtered and the filtrate was evaporated at 50° C. under vacuum to provide 10.6 g (100%) of product, as a gum.

来源