反应 #41355

反应方程式

Sodium periodate

3-phenoxy-1,2-propanediol

→

subtitle compound

收率 100.0%

2-Phenoxyacetaldehyde

收率 100.0%

溶剂

dichloromethane

dichloromethane

反应条件

后处理

1. 1
   过滤was filtered
2. 2
   浓缩the filtrate was concentrated

实验过程

Sodium periodate (0.65 M in water, 20 mL) was added to a vigorously stirred suspension of silica gel (20 g) in dichloromethane (160 mL), followed by a solution of 3-phenoxy-1,2-propanediol (1.68 g, 10.0 mmol) in dichloromethane (20 mL). After stirring for 10 min the mixture was filtered and the filtrate was concentrated to give the subtitle compound (1.36 g, 100%).

来源