反应 #40339

ord-0f91e36356c443afb325cec8d55ab4f8

反应方程式

CC(C)(C)OC(=O)N1CCC(=O)CC1
4-oxo-piperidine-1-carboxylic acid tert-butyl ester
CC(C)C1CCC(=O)C(Br)C1
2-bromo-4-isopropyl-cyclohexanone
CC(C)(C)OC(=O)N1CCC(=O)C(Br)C1
title compound
CC(C)(C)OC(=O)N1CCC(=O)C(Br)C1
3-bromo-4-oxo-piperidine-1-carboxylic acid tert-butyl ester

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

The bromination of 4-oxo-piperidine-1-carboxylic acid tert-butyl ester takes place in a manner similar to that described above for the preparation of 2-bromo-4-isopropyl-cyclohexanone. The title compound is reacted as a crude product without further characterization.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07727979B2uspto-grants-2010_06