反应 #40329

反应方程式

8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]dec-7-ene

hydrogen

→

8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]decane

反应条件

实验过程

8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]dec-7-ene is hydrogenated using Pd/C with hydrogen. After filtering-off of the catalyst over celite and evaporating-off of the solvent, 8-(4-fluorophenyl)-1,4-dioxaspiro[4.5]decane is obtained in a quantitative yield: tR 3.65 min (LC-1); ESI-MS(+): m/z 237.26 [M+H]+.

来源