反应 #40287

ord-128be03e30fc479198b6496eaff8785b

反应方程式

CCOC(=O)CON
2-Aminoxy-acetic acid ethyl ester
C#CCCC(=O)O
4-Pentynoic acid
C(=NC1CCCCC1)=NC1CCCCC1
dicyclohexylcarbodiimide
C#CCCC(=O)NOCC(=O)OCC
Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester

溶剂

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

To a solution of 2-Aminoxy-acetic acid ethyl ester (573 mg, 4.8 mmol) and 4-Pentynoic acid (441 mg, 4.5 mmol) in 15 mL EtOAc were added dicyclohexylcarbodiimide (928 mg, 4.5 mmol) and the resulting mixture was stirred at room temperature for 16 h.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07727713B2uspto-grants-2010_06