反应 #40284

反应方程式

N-Boc-β-alanine

propargyl alcohol

Dicyclohexyl-carbodiimide

→

N-Boc-β-alanine Propargyl Ester

溶剂

EtOAc

反应条件

后处理

1. 1
   过滤the reaction mixture was filtered
2. 2
   其他evaporated to dryness under vacuum
3. 3
   其他Crude product yield

实验过程

N-Boc-β-alanine (1.91 g, 10.1 mmol) and propargyl alcohol (0.675 g, 12 mmol) were dissolved in EtOAc (25 mL). Dicyclohexyl-carbodiimide (DCC, 2.06 g, 10 mmol) was added to the solution and after 16 h of stirring at room temperature, the reaction mixture was filtered and evaporated to dryness under vacuum. Crude product yield

来源