反应 #3738

ord-712a4c23c26a4619a1659f080875532d

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

The title compound was prepared from 1,3-di-cyclohexylmethyl-8-nitro xanthine (1 g, 0.0026 mol) and concentrated hydrobromic acid (40 ml, 48%) over 32 hours using an analogous procedure to that described in Example 15. The title product was obtained as a crystalline solid, m.pt. 247° C.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05734051uspto-grants-1998_03