反应 #367110

反应方程式

L-arabinose

hydrazine hydrate

→

L-arabinose hydrazone

溶剂

methanol

反应条件

后处理

1. 1
   其他evaporated in vacuo
2. 2
   workup.ADDITIONA 5 ml portion of methanol was added to the residue
3. 3
   其他The solid was collected
4. 4
   其他dried

实验过程

A solution of 2.0 g of L-arabinose in 5 ml of methanol and 5 ml of hydrazine hydrate was stirred overnight and then evaporated in vacuo. A 5 ml portion of methanol was added to the residue. After standing overnight the oil solidified. The solid was collected and dried, giving 1.5 g of L-arabinose hydrazone.

来源