反应 #348459

反应方程式

4-allyl-3-methyl-2,6-dinitrochlorobenzene

xylene

3-hexylamine

water

→

N-(3-Hexyl)-4-allyl-3-methyl-2,6-dinitroaniline

反应条件

后处理

1. 1
   温度The mixture is refluxed for 5 hours
2. 2
   洗涤The organic phase is washed with 5% hydrochloric acid
3. 3
   干燥water, dried over calcium sulfate
4. 4
   其他removed in vacuo
5. 5
   其他to leave the above-named product

实验过程

One equivalent of 4-allyl-3-methyl-2,6-dinitrochlorobenzene is dissolved in three volumes of xylene containing two equivalents of 3-hexylamine. The mixture is refluxed for 5 hours and then poured into water. The organic phase is washed with 5% hydrochloric acid and then water, dried over calcium sulfate, and removed in vacuo to leave the above-named product.

来源