反应 #318648

反应方程式

N-allylcyclohexylamine

1,1,3,3-tetramethyldisiloxane

→

1,3-bis(N-cyclohexyl-3-aminopropyl)-1,1,3,3-tetramethyldisiloxane

反应条件

后处理

1. 1
   workup.DISTILLATIONThe product, in nearly quantitative yield, is purified by vacuum distillation at <1 torr at a temperature of 207°-210° C.

实验过程

Following the technique described in Example 1, N-allylcyclohexylamine (0.173 mole), 1,1,3,3-tetramethyldisiloxane (0.0783 mole), and 0.05 g hexachloroplatinic acid are stirred at 70° C. for eight hours at 110° C. under nitrogen. The product, in nearly quantitative yield, is purified by vacuum distillation at <1 torr at a temperature of 207°-210° C.

来源