反应 #312585
ord-e340a01c97f3477caf8d844c91753b25
反应条件
详细条件
See reaction.notes.procedure_details.
后处理
- 1其他separated into two layers
实验过程
88.2 g (0.44 mole) of phenacyl bromide and 39.1 g (0.44 mole) of tetrahydrothiophene were dissolved in 220 g of nitromethane, which was stirred for 4 hours at room temperature. 800 g of water and 400 g of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, phenacyltetrahydrothiophenium bromide.