反应 #312584

ord-22bb0ac316144d56bcc523fe31a5b87e

溶剂

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他The target compound was obtained
  2. 2
    其他the procedure of Synthesis Example 1 aside
  3. 3
    其他in Synthesis Example 1
  4. 4
    萃取for extraction

实验过程

The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-tert-butylphenyl)sulfoxide instead of the diphenyl sulfoxide and 4-tert-butylbromobenzene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07556909B2uspto-grants-2009_07