反应 #3062

ord-53859d19f5084c73a9229630dac0c84d

反应方程式

COC(=O)CNCC(=O)OC.Cl
iminodiacetic acid dimethylester hydrochloride salt
CCN(C(C)C)C(C)C
N,N-diisopropyl-ethylamine
BrCCCBr
1,3-dibromopropane
COC(=O)CN(CCCBr)CC(=O)OC
title compound
COC(=O)CN(CCCBr)CC(=O)OC
Dimethyl N-(3-Bromopropyl)iminodiacetate

溶剂

反应条件

温度
90°CELSIUS
详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他chromatographed

实验过程

A mixture of 1 mmol iminodiacetic acid dimethylester hydrochloride salt, 5 mmol N,N-diisopropyl-ethylamine and 3 mmol 1,3-dibromopropane in 2 mL toluene was stirred at 90° C. for 16 h and then chromatographed to provide the title compound as an oil.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US05731432uspto-grants-1998_03