反应 #2507846

ord-98c3198f70774fed8176f88e3b49eb54

反应方程式

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene
→
NCC(=O)O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
Trehalose Glycine

反应物

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene

试剂

无

溶剂

O
water
O
water

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    workup.ADDITIONwas added at room temperature
  2. 2
    其他was obtained
  3. 3
    workup.ADDITIONWithout adding any acid

实验过程

17.84 g of trehalose dihydrate and 4.03 g of glycine were carefully weighed and transferred into a sterile polypropylene bottle, to which 300 ml of purified water was added at room temperature and stirred slowly until a clear solution was obtained. The pH was measured and found to be 5.5. Without adding any acid, the volume was adjusted to 350 ml with purified water. The pH was measured and found to be 5.5.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US07956028B2uspto-grants-2011_06