反应 #2467932
ord-1931052940a24382be4e0266350ed35a
反应方程式
sodium hydroxide
melamine
dimethoxyethanal
→
Melamine Dimethoxyethanal
反应条件
温度
52.5°CELSIUS
详细条件
See reaction.notes.procedure_details.
后处理
- 1温度This mixture was heated
- 2温度while maintaining the pH
- 3其他close to 9-9.5 with adjustment
实验过程
200 g of melamine (1.59 mol) were added to 660 g of a 60% aqueous solution of dimethoxyethanal (3.81 mol). This mixture was heated under stirring for 2 h at 50-55° C. while maintaining the pH close to 9-9.5 with adjustment, if necessary, with as much 20% sodium hydroxide as was required (about 7 g).