反应 #2460345

反应方程式

Ethyl-(3-nitropyridin-4-yl)amine

→

title compound

收率 94.0%

N4-ethylpyridine-3,4-diamine

收率 94.0%

溶剂

ethanol

反应条件

后处理

1. 1
   过滤After filtration of the catalyst through celite
2. 2
   浓缩the filtrate was concentrated in vacuo

实验过程

Ethyl-(3-nitropyridin-4-yl)amine (8.7 g, 52.0 mmol) in ethanol (150 ml) was hydrogenated for 18 hours in the presence of 10% palladium on carbon. After filtration of the catalyst through celite, the filtrate was concentrated in vacuo to afford the title compound (6.7 g, 94%).

来源