反应 #2389089

反应方程式

dodecane thiol

sulfuryl chloride

→

dodecansulfenyl chloride

溶剂

CHCl3

反应条件

后处理

1. 1
   其他Removal of solvent (aspirator)

实验过程

To a solution of dodecane thiol (1.00 mL, 4.17 mmol, Aldrich Chemical Company) in 20 mL CHCl3 was added sulfuryl chloride (0.74 mL, 9.18 mmol, Aldrich Chemical Company), and the resulting mixture was stirred at room temperature for 18 h. Removal of solvent (aspirator), afforded dodecansulfenyl chloride that was determined to be sufficiently pure by 1H NMR.

来源