反应 #2389088

反应方程式

dodecane thiol

chloride

→

dodecansulfenyl chloride

溶剂

CHCl3

反应条件

后处理

1. 1
   其他Removal of solvent (aspirator)

实验过程

To a solution of dodecane thiol (1.00 mL, 4.17 mmol, Aldrich) in 20 mL CHCl3 was added suliryl chloride (0.74 mL, 9.19 mmol, Aldrich), and the regulting mixture was stirred at room temperature for 18 h. Removal of solvent (aspirator), afforded dodecansulfenyl chloride that was determined to be sufficiently pure by 1H NMR.

来源