反应 #2389085

反应方程式

9-Hydroxyphenalenone

aluminum chloride

→

Tris (9-oxidophenalenone) aluminum

溶剂

toluene

反应条件

后处理

1. 1
   其他to form
2. 2
   温度The flask was then cooled
3. 3
   过滤the contents filtered

实验过程

9-Hydroxyphenalenone (1.5 g) was placed in a 100 mL round-bottom flask. Dry toluene (50 mL) was added to the flask together with aluminum chloride (0.113 g). The solution turned yellow-orange, and a precipitate began to form. The mixture was refluxed at 110° C. overnight. The flask was then cooled and the contents filtered. Crude yield 1.69 g, mp>300° C.

来源