反应 #2328994

反应方程式

2-(6-bromopyridin-3-yl)-6-methoxy-1,3-benzoxazole

3-bromo-6-formylpyridine

→

title compound

2-(5-Bromopyridin-2-yl)-6-methoxy-1,3-benzoxazole

反应条件

后处理

1. 1
   其他to give 578.1 mg as an off white solid

实验过程

The title compound was synthesized according to a procedure similar to that as described for 2-(6-bromopyridin-3-yl)-6-methoxy-1,3-benzoxazole starting from 3-bromo-6-formylpyridine to give 578.1 mg as an off white solid: 1H NMR δ ppm 8.91 (dd, 1H) 8.26-8.32 (m, 1H) 8.20 (dd, 1H) 7.75 (d, 1H) 7.46 (d, 1H) 7.06 (dd, 1H) 3.86 (s, 3 H); MS m/z 305, 307 (M+H, Bromo isotopes).

来源