反应 #2320120

ord-c0d67ae504ee45ada20edc0cf0df026e

反应方程式

CS(=O)(=O)c1cc(Br)ccc1Cl
5-bromo-2-chloro-methanesulfonyl-benzene
C1CNCCN1
piperazine
CS(=O)(=O)c1cc(N2CCNCC2)ccc1Cl
1-(4-Chloro-3-methanesulfonyl-phenyl)-piperazine

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他the title compound was recovered by the procedure

实验过程

Beginning with 5-bromo-2-chloro-methanesulfonyl-benzene and piperazine, the title compound was recovered by the procedure described in Example 1. MS m/z (rel. intensity, 70 eV)) 274 (M+, 20), 234 (40), 232 (bp), 153 (9), 56 (12).

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: USRE041315E1uspto-grants-2010_05