反应 #2320116

ord-977ef84577d2439fbb7cbd128d3f00bf

反应方程式

Clc1ccc(Br)cc1Cl
4-bromo-1,2-dichlorobenzene
C1CNCCN1
piperazine
Clc1ccc(N2CCNCC2)cc1Cl
title compound
收率 48.2%
Clc1ccc(N2CCNCC2)cc1Cl
1-(3,4-dichloro-phenyl)-piperazine
收率 48.2%

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

Beginning with 4-bromo-1,2-dichlorobenzene (200 mg, 0.88 mmol) and piperazine (91 mg, 1.06 mmol), 98 mg of the title compound was recovered by the procedure described in Example 1.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: USRE041315E1uspto-grants-2010_05