反应 #2320107

ord-5edfabeda1e84341a10f3b54fab6d6df

反应方程式

CCCN1CC=C(c2ccc(N)c(C(F)(F)F)c2)CC1
4-(1-Propyl-1,2,3,6-tetrahydropyridine-4-yl)-2-trifluoromethyl-phenylamine
CCCN1CCC(c2ccc(N)c(C(F)(F)F)c2)CC1
4-(1-Propyl-piperidin-4-yl)-2-trifluoromethyl-phenylamine

溶剂

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他the titled compound was recovered by the procedure
  2. 2
    其他described in Preparation 6

实验过程

Beginning with 4-(1-Propyl-1,2,3,6-tetrahydropyridine-4-yl)-2-trifluoromethyl-phenylamine, the titled compound was recovered by the procedure described in Preparation 6: MS m/z (rel. intensity, 70 eV)) 286 (M+, 2), 257 (17), 98 (10), 96 (8), 70 (bp), Rf=0.28 (MeOH).

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: USRE041315E1uspto-grants-2010_05