反应 #2320102

反应方程式

5-bromo-2-chlorobenzotrifluoride

cis-2,6-dimethyl-1-propyl-piperazine

HCl

→

cis-4-(4-Chloro-3-trifluoromethyl-phenyl)-2,6-dimethyl-1-propyl-piperazine

反应条件

后处理

1. 1
   其他the title compound was recovered by the procedure
2. 2
   其他described in Preparation 9

实验过程

Beginning with 5-bromo-2-chlorobenzotrifluoride and cis-2,6-dimethyl-1-propyl-piperazine, the title compound was recovered by the procedure described in Preparation 9: m.p. 256° C. (HCl), MS m/z (rel. intensity, 70 eV)) 335 (M+, 5), 305 (55), 112 (bp), 70 (67), 56 (82).

来源