反应 #2320092

ord-593d0bd1bb5a43e290134658a3df1db2

反应方程式

Fc1cc(N2CCNCC2)cc(C(F)(F)F)c1
1-(3-fluoro-5-trifluoromethyl-phenyl)-piperazine
CCCBr
1-bromopropane
CCCN1CCN(c2cc(F)cc(C(F)(F)F)c2)CC1
1-(3-Fluoro-5-trifluoromethyl-phenyl)-4-propyl-piperazine

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他the title compound was recovered by the procedure

实验过程

Beginning with 1-(3-fluoro-5-trifluoromethyl-phenyl)-piperazine and 1-bromopropane, the title compound was recovered by the procedure described in Example 2. m.p. 242° C. (HCl); MS m/z (rel. intensity, 70 eV) 290 (M+, 34), 261 (bp), 218 (22), 190 (20), 70 (37).

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: USRE041315E1uspto-grants-2010_05