反应 #2320090

ord-1feed4a1abe548b7aee54b3244900d71

反应方程式

O=[N+]([O-])c1cc(N2CCNCC2)ccc1Cl
1-(4-Chloro-3-nitro-phenyl)-piperazine
CCCBr
1-bromopropane
CCCN1CCN(c2ccc(Cl)c([N+](=O)[O-])c2)CC1
1-(4-Chloro-3-nitro-phenyl)-4-propyl-piperazine

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他the title compound was recovered by the procedure

实验过程

Beginning with 1-(4-Chloro-3-nitro-phenyl)-piperazine and 1-bromopropane, the title compound was recovered by the procedure described in Example 2. m.p. 249° C. (HCl); MS m/z (rel. intensity, 70 eV) 283 (M+, 27), 254 (87), 165 (bp), 153 (78), 56 (90).

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: USRE041315E1uspto-grants-2010_05