反应 #2314313

ord-874be716e65d480aa5a1a5e256a07d9a

反应方程式

OCCc1ccccc1
2-Phenylethanol
C=Cc1ccc(S(=O)(=O)Cl)cc1
p-styrene sulfonyl chloride
CCN(CC)CC
triethylamine
C=Cc1ccc(S(=O)(=O)OCCc2ccccc2)cc1
desired product
C=Cc1ccc(S(=O)(=O)OCCc2ccccc2)cc1
2-Phenylethyl p-Styrene Sulfonate

反应条件

详细条件
See reaction.notes.procedure_details.

实验过程

2-Phenylethanol (3.1 g) was reacted with p-styrene sulfonyl chloride (5.3 g) and triethylamine (2.7 g) in 20 ml of dichloromethane for 3 hours to give the desired product as a light yellow viscous oil that was purified by passing through basic aluminum oxide.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US06413694B1uspto-grants-2002_07