反应 #2314299

反应方程式

potassium carbonate

4-octyloxy-4′-tetrahydropyranyloxybiphenyl

toluenesulfonic acid

→

4-hydroxy-4′-octyloxybiphenyl

溶剂

methanol

反应条件

后处理

1. 1
   workup.ADDITIONis added
2. 2
   过滤is then filtered
3. 3
   其他The solvent is removed in vacuo

实验过程

To a solution of 4-octyloxy-4′-tetrahydropyranyloxybiphenyl 9E (R=octyl) (5 g) in methanol (39 ml) is added toluenesulfonic acid (25 mg). The reaction mixture is stirred at room temperature overnight, at which time potassium carbonate (1 g) is added. The reaction mixture is stirred an additional hour, and is then filtered. The solvent is removed in vacuo.

来源