反应 #2314297

ord-6e28400805e2472eb1dc17fc3e192c40

反应方程式

Oc1ccc(-c2ncc(OCc3ccccc3)cn2)cc1
5-benzyloxy-2-(4-hydroxyphenyl)pyrimidine
CCCCCCCCCCBr
bromodecane
CCCCCC1=CCC(COc2ccc(CCC3CC=C(CCC=C(C)C)CC3)cc2)CC1
ether
CCCCCC1=CCC(COc2ccc(CCC3CC=C(CCC=C(C)C)CC3)cc2)CC1
4-[2-(4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)ethyl]-1-(4-pentyl-3-cyclohexenyl)methoxybenzene
CCCCCCCCCCOc1ccc(-c2ncc(OCc3ccccc3)cn2)cc1
5-benzyloxy-2-(4-decyloxyphenyl)pyrimidine

反应条件

详细条件
See reaction.notes.procedure_details.

后处理

  1. 1
    其他prepared essentially

实验过程

The reaction between 5-benzyloxy-2-(4-hydroxyphenyl)pyrimidine (prepared essentially according to the procedure of E. P. Janulis et al., U.S. Pat. No. 5,399,291) and bromodecane is essentially that used for synthesis of ether 2H.

来源

DOI: 10.6084/m9.figshare.5104873.v1专利: US06413448B1uspto-grants-2002_07