反应 #2314285

反应方程式

water

boron tribromide

anisole

2-(4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)ethyl-4-methoxybenzene

→

4-[2-(4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)ethyl]phenol

溶剂

dichloromethane

反应条件

后处理

1. 1
   萃取The reaction mixture is extracted with dichloromethane
2. 2
   干燥dried over magnesium sulfate
3. 3
   浓缩The solution is concentrated in vacuo
4. 4
   其他The product is recrystallized from hexane

实验过程

To a solution of anisole 2F (R=4-Methyl-3-pentenyl) (6 g) in dichloromethane (100 mL) and cooled in an ice bath is added a 1M solution of boron tribromide (3.4 mL). The solution is stirred for one hour, then poured into water. The reaction mixture is extracted with dichloromethane and dried over magnesium sulfate. The solution is concentrated in vacuo. The product is recrystallized from hexane.

来源