反应 #2267059

反应方程式

tetramethylammonium hydroxide

pentafluorobenzenesulfonyl chloride

→

tetramethylammonium pentafluorobenzenesulfonate

溶剂

methanol

反应条件

后处理

1. 1
   workup.ADDITIONwas slowly added

实验过程

In 100 ml of methanol was dissolved 25 g of pentafluorobenzenesulfonyl chloride under cooling with ice, and 100 g of an aqueous solution of 25% tetramethylammonium hydroxide was slowly added thereto. The mixture was stirred for 3 hours at room temperature to obtain a solution of tetramethylammonium pentafluorobenzenesulfonate. The solution was used for salt-exchange with a sulfonium salt or an iodonium salt.

来源